Mass Spectrometry

Precise Mass


Modern high-resolution mass spectrometers are capable of determining very precise molecular weights of substances. Whereas the chemical methods introduced earlier (vapor density method, cryoscopic method, vapor pressure osmometry, and neutralization equivalent) are accurate to within 0.1 to 1% (two or three significant figures), the mass spectrometer has an accuracy of 0.005%.

What does this mean? To illustrate, a molecule with a molecular weight of 60 could be C3H8O, C2H8N2, C2H4O2, or CH4N2O. These compounds would have precise masses as follows:

C3H8O 60.05754
C2H8N2 60.06884
C2H4O2 60.02112
CH4N2O 60.03242

These precise masses are calculated using the precise masses of the elements given in the table below.

Element Atomic Weight Nuclide Mass
Hydrogen 1.00797 1H 1.00783
    2H 2.01410
Carbon 12.01115 12C 12.0000
    13C 13.00336
Nitrogen 14.0067 14N 14.0031
    15N 15.0001
Oxygen 15.9994 16O 15.9949
    17O 16.9991
    18O 17.9992
Fluorine 18.9984 19F 18.9984
Silicone 28.086 28Si 27.9769
    29Si 28.9765
    30Si 29.9738
Phosphorus 30.974 31P 30.9738
Sulfur 32.064 32S 31.9721
    33S 32.9715
    34S 33.9679
Chlorine 35.453 35Cl 34.9689
    37Cl 36.9659
Bromine 79.909 79Br 78.9183
    81Br 80.9163
Iodine 126.904 127I 126.9045

 


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